Synthesis and Characterization of thermo physical properties of phthalic anhydride glycerol Resin (PAGR) from soybean oil
Keywords:
Alcoholysis method, phthalic anhydride glycerol Resin, soybean oil, Pentaerthritol and lithargeAbstract
Phthalic anhydride-glycerol Resin(PAGR) increase the flexibility of paint, resist to acid rain effect, increases the adhesiveness, brushing power, film hardness, layer flexibility, durability, gloss retention, resistance to abrasion also helps to decrease the overall drying time of paints. Phthalic anhydride-glycerol Resin is produced by reacting polyfunctional alcohol with the poly basic and monofunctional acid by Alcoholysis process. Moreover, Phthalic anhydride-glycerol Resin(PAGR) is a major raw material for coatings, varnishes and binders. Phthalic anhydride-glycerol Resin(PAGR) is used in paints coating compositions, adhesive, plastics, varnishes, printing ink, floor coverings. In the present research work, Phthalic anhydride-glycerol Resin is synthesized using soybean oil, pentaerythritol, phthalic anhydride and litharge (PbO). It was further characterized by FTIR ,DSC TGA and acid value
References
Tapan Kanai, T.K. Mahato, Dhirendra Kumar, Synthesis and characterization of novel silicone acrylate–soya alkydresin as binder for long life exterior coatings, Progress in Organic Coatings 58 (2007) 259–264 .
Frank et al "Alkyd Resins" in Ullmann`s Encyclopedia of Industrial Chemistry, Wiley-VCH, Weinheim, 2005.
E.U. Ikhuoria , M. Maliki , Synthesis and characterisation of chlorinated rubber seed oil alkyd resins, Progress in Organic Coatings 59 (2007) 134–137.
Waters, R.T. Resins Synthetic, s Alkyd Resins, section 2. London Wyman and son1995.
Additives for Coatings" J. H. Bielman, Ed. Wiley-VCH, 2000, Weinheim.
Ikhouria E.U.,Aigbodion, A.I., AND OKIEIMEN F.F Enhancing the quality of Alkyd Resins using Methyl Ester of rubber oil Seed” Triocal Journal of pharmaceutical Research 3. Vol. 3 (1) 2004: 311-317.
Edwin A. Murillo, Synthesis and characterization of hyper branched alkyd resins based on tall oil fatty acids, Progress in Organic Coatings 69 (2010) 235–240.
Kirk, encyclopedia of chemical engineering vol.2, 2010.
Snaler, S.R et al. polymer synthesis and characterization. A laboratory manual USA Academic press . California 1998.
Pirita Uschanov, Nina Heiskanen Synthesis and characterization of tall oil fatty acids-based alkyd resins and alkyd–acrylate copolymers, Progress in Organic Coatings 63 (2008) 92–99.
J.S LONG, Filming forming composition, vol 1 New York (1967)72-82.
Mehlenbancher V.C Official and Testing Methods for the American oil chemists Society Chicago: 35 east Wacker Drive 1950.
Serdar, Aydin, Hu¨seyin Akc,ay,vThe effects of anhydride type and amount on viscosity and film properties of alkyd resin, Progress in Organic Coatings 51 (2004) 273–279.
Rebecca Ploeger, Thermal analytical study of the oxidative stability of artists’ alkyd paints Polymer Degradation and Stability Volume 94, (2009)2036-2041.
G.Guclu, alkyd resin synthesized from PET bottles progress in organic coating 65(2009)362-365.
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